Fabrication of Selective and Sensitive Hydrazine Sensor Using Sol-Gel Synthesized MoSe2 as Efficient Electrode Modifier

نویسندگان

چکیده

Due to its hazardous nature, the determination of hydrazine is great significance. This study designed and fabricated a electrochemical sensor. Two-dimensional (2-D) molybdenum diselenide (MoSe2) has been synthesized by using sol-gel method. The phase purity formation MoSe2 was determined powder X-ray diffractometer. surface morphological characteristics were studied scanning electron microscopy. presence Mo Se elements in checked energy dispersive spectroscopy. glassy carbon (GC) electrode (3 mm) modified with prepared via drop-cast approach. MoSe2-glassy (MoSe2-GC) used as working for sensing application. properties MoSe2-GC analyzed linear sweep voltammetry cyclic voltammetry. shown sensitivity 0.68 µA/µMcm2 detection limit 0.091 µM. In addition, also good selectivity toward various interfering compounds. excellent electro-catalytic behavior solely responsible this enhanced performance MoSe2-GC.

برای دانلود رایگان متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Fabrication of a Selective and Sensitive Electrochemical Sensor Modified with Magnetic Molecularly Imprinted Polymer for Amoxicillin

A modified electrochemical sensor for the determination of amoxicillin (AMX) was reported in this paper. The magnetic molecularly imprinted polymer (MMIP) were suspended in AMX solution and then collected on the surface of a magnetic carbon paste electrode (CPE) via a permanent magnet, situated within the carbon paste electrode and then the voltammetry signals were recorded. It was confirmed th...

متن کامل

Fabrication of Ultraviolet Photodetector Based on ZnO Nanostructures and Calcium Impurities Using Sol-Gel Method

In this paper an ultraviolet (UV) photodetector has been fabricated using ZnO nanostructures. The cheap fabrication process, high-quality nanostructures and the desired results for the photodetector are the most important characteristics of the proposed method. ZnO nanostructures have been grown using sol-gel method. In order to increase the sensitivity, calcium impurities have been added to na...

متن کامل

Structure and luminescence of sol-gel synthesized anatase nanoparticles

Two samples of mesoporous anatase nanoparticles, prepared by the sol-gel method, were characterised by Cs-corrected high resolution transmission electron microscopy (HRTEM), X-ray powder diffraction (XRD) and Raman spectroscopy. Statistical evaluation of TEM data showed an average diameter of these crystallites of 8.8 nm and 11.1 nm, respectively. Optical spectroscopy by cathodoluminescence (CL...

متن کامل

The Sonogel-Carbon electrode as a sol-gel graphite-based electrode.

In this work, a novel sol-gel-based procedure to obtain solid carbon composite electrodes is proposed. The procedure is based on the use of sonocatalysis to apply high-energy ultrasound directly to the precursors; this way, ultrasonic cavitation is achieved so that hydrolysis with acidic water is promoted in the absence of any additional solvent and the time needed to get a unique phase is redu...

متن کامل

Controlled deposition of sol–gel sensor material using hemiwicking

Optical sensors are fabricated by depositing liquid sol–gel sensor material on a polycarbonate surface, which has been decorated with arrays of periodic micropillars. Using the principle of hemiwicking, the liquid material is spread, guided by the surface structures, to homogeneously fill the volume between the surface structures and form a liquid film with a thickness determined by the height ...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

ژورنال

عنوان ژورنال: Crystals

سال: 2023

ISSN: ['2073-4352']

DOI: https://doi.org/10.3390/cryst13020161